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OVERVIEW
DOWNLOADS
Brand: CEM
Part No: PHOENIX
Availability: 6-8 weeks

Speed, Capacity, Versatility

Phoenix
Microwave
Muffle 
Furnace

 

Precise Results in Seconds

 

The Phoenix line of microwave muffle furnaces offers unmatched versatility and speed in a rugged, easy-to-use system. Choose from two configurations and a variety of options!
 

Legendary power at your fingertips!
 

  • Convenience - Accurate results in minutes
  • Speed - Up to 10 times faster than conventional muffle furnaces
  • Capacity - Ash up to 15 samples at one time
  • Versatility - Use any type of crucible normally used in conventional ashing systems, even platinum


The Phoenix Microwave Muffle Furnace System is available with your choice of either a High Temperature or High Capacity furnace. The High Temperature furnaces reach 1,200 °C and can process up to eight 25-mL crucibles. For laboratories needing greater throughput, the High Capacity furnaces reach 1,000°C and hold up to fifteen 25-mL crucibles. Any crucible that can be used in a conventional muffle furnace (including platinum) can also be used in the Phoenix Microwave Muffle Furnace Systems.

 

Phoenix™ Microwave Muffle Furnace

The Phoenix Microwave Muffle Furnaces enable companies in many diverse industries to improve their process control, allowing them to make rapid adjustments to reduce "out-of-specification" product. These systems can perform many high temperature applications up to 97% faster than traditional muffle furnaces. The standard Phoenix Microwave Muffle Furnace configuration features:
 

  • Programmable temperature control
  • Auto-Start/Auto-Shutdown software
  • Built-in exhaust system
  • Entry and storage of up to 20 methods
  • Built-in calibration software
  • Over-temperature and thermocouple failure safeguards
  • Built-in system diagnostics
  • Use any type of crucible normally used in a conventional muffle furnace, including platinum!


The Phoenix Microwave Muffle Furnace Systems are rugged, easy-to-use and engineered to be dependable. Temperature verification and temperature calibration for ISO and GLP practices are quickly and easily performed with optional accessories including NIST traceable dual thermocouples and calibration source instruments.

 

Phoenix satisfies the equipment requirements for "electrically heated" furnaces in the following methods:

* ASTM, USP (281 - ROI & 733-LOI), AOAC, FDA, ISO & DIN

Phoenix also meets the requirements for applications listing a "microwave-heated" furnace

* ASTM D5630-94, ASTM D1506-94b

 

Workstation

All Phoenix Microwave Muffle Furnace Systems are available with workstation options including a balance and printer.

The Phoenix Workstation option transforms your microwave muffle furnace into a complete center for accurate ashing and data compilation. The system utilizes the furnace’s built-in serial and parallel ports to connect to a balance for weighing and a printer for complete documentation of the ashing process to assist you in complying with ISO and other QC requirements.

The Phoenix Workstation uses a 100 g balance with 0.0001 g sensitivity for sample weighing. The balance communicates directly with the Phoenix furnace by a RS-232 port, which is a standard feature in every CEM muffle furnace. Once the sample has completed the ashing process and has been reweighed, the user can choose to print the sample results and information with the Workstation’s printer.

 

Phoenix Features

Fast & Efficient
Phoenix Microwave Muffle Furnaces perform many high temperature applications up to 97% faster than traditional muffle furnaces, giving you more time to make adjustments to your process and reduce out-of-specification product.


Safe
Phoenix reduces exposure to fumes and heat with a built-in exhaust system that does not require fume hood space. These rugged, durable furnaces features door interlocks and built-in system diagnostics.

Accurate
Phoenix Microwave Muffle Furnaces satisfy standard methods that require electrically heated furnaces. They have built-in calibration software and NIST traceable accessories are available.


Easy-to-Use
Auto-start software allows pre-programmable warm-up and shut down. Phoenix Microwave Muffle Furnaces store up to 20 user-programmed methods.

 

Phoenix Sulfated Ashing

Ash pharmaceutical raw materials, excipients and finished products in minutes, while safely removing and neutralizing sulfur dioxide and nitric acid emissions to meet ISO 14000 regulations. The Phoenix Microwave Sulfated Ashing Option features a vapor scrubber system to safely remove harmful fumes from the furnace cavity and neutralize any residual acid exhausted from the sulfated ashing process.

  • Meets requirements for USP 281 (ROI) & USP 733 (LOI)
  • Built-in serial and parallel ports provide full documentation of method, completion date, and time
  • Menu-driven software permits simple entry and storage of operating parameters for up to 20 methods
  • Rapid disconnect feature allows system to be used as either a standard ashing system or a sulfated ashing system in less than 5 minutes without the use of tools
  • Quartz furnace ceiling assures sample purity
  • Easy-to-use
  • Available as a workstation with balance and printer


Temperature verification and temperature calibration for ISO and GLP practices are quickly and easily performed with optionalaccessories including NIST traceable dual thermocouples and calibration source instruments.

 

Phoenix Airwave

The Phoenix Airwave Microwave Muffle Furnace meets the most demanding requirements of large organic samples with ease. This microwave muffle furnace utilizes a patented air amplified exhaust system to quickly and safely ash samples, removing large quantities of air and volatile by-products.

Legendary power at your fingertips!

  • Fast, accurate, easy-to-use
  • Eliminates the need for volume reduction/carbonization on a Bunsen burner or hot plate
  • Exhaust 130 CFM or more of air per minute (adjustable)
  • Volume reduction of large samples in minutes by high-speed evaporation
  • Increased airflow accelerates oxidation of samples


The Phoenix Airwave Microwave Muffle Furnace is available with your choice of either a High Temperature or High Capacity furnace. The High Temperature furnaces reach 1,200 °C and can process up to eight 25-mL crucibles. For laboratories needing greater throughput, the High Capacity furnaces reach 1,000 °C and hold up to fifteen 25-mL crucibles. Any crucible that can be used in a conventional muffle furnace (including platinum) can also be used in the Phoenix Microwave Ashing Systems.

Standard features include:

  • Programmable temperature control
  • Auto-Start/Auto-Shutdown software
  • Built-in exhaust system
  • Entry and storage of up to 20 methods
  • Built-in calibration software
  • Over-temperature and thermocouple failure safeguards
  • Built-in system diagnostics
  • Use any type of crucible normally used in a conventional muffle furnace, including platinum!
  • Available as a workstation with balance and printer


The Phoenix Airwave Microwave Muffle Furnace can perform many high temperature applications up to 97% faster than conventional muffle furnaces. The system is rugged and engineered to be dependable. Temperature verification and temperature calibration for ISO and GLP practices are quickly and easily performed with optional accessories including NIST traceable dual thermocouples and calibration source instruments.

 

Phoenix Bone Content Analysis

Direct bone content analysis in less than 15 minutes!

Forget titrations and back calculations for bone content! Get a fast, accurate and direct bone content analysis with the PhoenixMicrowave Furnace. Save money and increase production yields by running closer to target!
 

Phoenix™ 
for Bone Content Analysis

  • Direct method
  • More accurate than titration
  • No chemicals
  • Accurate bone content in less than 15 minutes!
  • Automatically calculates results

 

Bone Content Results: Mechanically Separated Chicken (MSC)

Sample % Bone AOAC Bone Difference
1 0.77 0.83 -0.06
2 0.70 0.76 -0.06
3 0.80 0.62 0.18
4 0.86 0.51 0.35
5 0.59 0.55 0.04
6 0.64 0.56 0.08
7 0.79 0.50 0.29
8 0.50 0.50 0
9 0.83 0.85 -0.02
10 0.85 0.88 -0.03

 

Phoenix Accessories 

CEM offers accessories for the calibration and verification of the temperature control circuitry to meet governmental regulations for various applications.

 

Improve Results with Quartz Fiber Crucibles 

CEM’s unique, patented quartz fiber crucibles dramatically reduce ashing times and cool in seconds. The quartz fiber material allows oxygen to circulate around the sample speeding combustion even with our unique crucible caps in place. 

  • Reduce analysis time by as much as 97%!
  • Cools in seconds
  • No need for desiccation
  • Speeds sample oxidation using a flow through advanced material design
  • Withstands temperatures up to 1,000 °C
  • Unbreakable


Crucible caps can be used with our 50- or 100-ml crucibles. Try them out next time you have to ash a sample that needs to be contained. 

Ideal for low ash samples and samples with high organic content

  • Contains the sample when ignition occurs
  • Reduces contamination
  • Improves accuracy on ROI and LOI determinations

 

Automatic replenishment programs, yearly contracts and volume pricing are available for quartz fiber crucibles. For more information and part numbers, please visit our Consumables page.

 

Self-Sealing Quartz Crucibles 
For oxygen-free ashing, self-sealing quartz crucibles are available. These crucibles can be used for Carbon Black determination in polyethylene and polypropylene and eliminate the need for slow, fragile tube furnaces.

 

Ashing under Inert Gas *
The super-fast muffle furnace allows the rapid determination of soot and carbon fibers and carbon nanotubes in polymers

The Phoenix can be used as a rapid plastic incinerator with inert gas atmosphere. This enables the rapid ashing of a variety of different plastics and rubbers, for the determination of soot or carbon content and the content of carbon nanotubes. The result: What previously took hours, is now achieved in minutes. The application areas for such plastics compounds are typically in the aircraft and automobile (bumpers, moldings, fittings, sinks, counter tops, finished parts, etc.) amongst others.

Since the material properties of plastic compounds depend essentially on its filler content, a rapid determination of this filler (carbon black, carbon fiber, carbon nanotubes, etc.) is required for an effective process control. Substantial cost savings can be made by a quick intervention in the current production process. With a conventional muffle furnace, polymer and filler are incinerated together in a crucible and thus the filler cannot be measured. The alternative is to use the Phoenix with an inert gas atmosphere such as a nitrogen purge.

Results are obtained in just 10 minutes. The heating muffle is purged with an inert gas such as nitrogen. The plastic polymer is carbonized and exits the crucible but the carbon-containing filler in the crucible remains. The built-in fan removes smoke, heat and fumes automatically, thus increasing the active safety at work.

 

Material Science
The inert gas option can also be used in a variety of applications related to material science. Various publications have highlighted the benefits of using microwave energy and we can now offer a solution for reactions requiring an inert atmosphere.
Microwave irradiation quickly applies the energy necessary to achieve high temperatures, enabling reactions to be performed quickly and efficiently. The instant power on / power off provides for a steep rise in temperature during the heating but also for a steep decline during the cooling resulting in high quality materials.

 

Microwave energy has been used for making materials such as: 
 

Quantum Dots
Zeolites
Metal Oxides

Metal Organic Frameworks
Gold, silver, and other metal nanomaterials
Nanocomposite materials

Nitride powders
Lithium ion materials



*CEM cannot fully guarantee an oxygen-free environment using this process.

 

Calibration Source Instrument (NIST traceable) 
The calibration source instrument and built-in system software allow rapid calibration of the temperature control circuitry of the Phoenix Microwave Ashing Systems. A NIST traceable certificate of calibration is supplied with the instrument.

 

Dual Element Thermocouple (NIST traceable) 
The type K Dual Element Thermocouple contains two thermocouples in one sheath. While one thermocouple controls the operating temperature, the second thermocouple can be connected to a digital thermometer to verify the accuracy of the controlling thermocouple. It is NIST traceable with a certificate of calibration. 

 

Cooling Fan 
The furnace cooling fan rapidly reduces heat to the starting temperature.

 

All Phoenix Microwave Ashing Systems are available with workstation options including a balance and printer. 

 

The Phoenix consists of a 1400 W microwave heating system containing a 5.0 liter (300 in3) chamber which can be heated to 1000 °C or a 1.8 liter (112.5 in3) chamber which can be heat to 1200 °C using microwave energy. The unit maintains 2.8 m(100 ft3) of air flow per minute through the microwave cavity to rapidly ash materials and remove combustion by-products. Internal temperature calibration software. Includes integral dual thermocouple Temperature Control System for either single set-point temperature or eight segmented ramping temperature control programs. Program storing, processing and reporting weight data and % Ash, % LOI, % ROI, % LOD, %Fixed, %Volatile and %Total Residue to the instrument display, printer or external computer.  Two RS232C 9-pin serial interfaces for option balance and external computer; one 25-pin parallel port for optional printer.  Accessory Starter Kit includes: 8 ft. exhaust hose with connector, clamp 90 degree elbow. (20) 20 mL & (4) 50 mL Quartz Fiber Ashing Crucibles, (4) 50 mL crucibles and 200 ashing disks, spare fuses, thermocouple, pedestal access tool, power cord and operation manual. Manufactured by CEM Corporation, ISO-9001 certified. 

OVERVIEW
DOWNLOADS
Brand: CEM
Part No: PHOENIX
Availability: 6-8 weeks

Speed, Capacity, Versatility

Phoenix
Microwave
Muffle 
Furnace

 

Precise Results in Seconds

 

The Phoenix line of microwave muffle furnaces offers unmatched versatility and speed in a rugged, easy-to-use system. Choose from two configurations and a variety of options!
 

Legendary power at your fingertips!
 

  • Convenience - Accurate results in minutes
  • Speed - Up to 10 times faster than conventional muffle furnaces
  • Capacity - Ash up to 15 samples at one time
  • Versatility - Use any type of crucible normally used in conventional ashing systems, even platinum


The Phoenix Microwave Muffle Furnace System is available with your choice of either a High Temperature or High Capacity furnace. The High Temperature furnaces reach 1,200 °C and can process up to eight 25-mL crucibles. For laboratories needing greater throughput, the High Capacity furnaces reach 1,000°C and hold up to fifteen 25-mL crucibles. Any crucible that can be used in a conventional muffle furnace (including platinum) can also be used in the Phoenix Microwave Muffle Furnace Systems.

 

Phoenix™ Microwave Muffle Furnace

The Phoenix Microwave Muffle Furnaces enable companies in many diverse industries to improve their process control, allowing them to make rapid adjustments to reduce "out-of-specification" product. These systems can perform many high temperature applications up to 97% faster than traditional muffle furnaces. The standard Phoenix Microwave Muffle Furnace configuration features:
 

  • Programmable temperature control
  • Auto-Start/Auto-Shutdown software
  • Built-in exhaust system
  • Entry and storage of up to 20 methods
  • Built-in calibration software
  • Over-temperature and thermocouple failure safeguards
  • Built-in system diagnostics
  • Use any type of crucible normally used in a conventional muffle furnace, including platinum!


The Phoenix Microwave Muffle Furnace Systems are rugged, easy-to-use and engineered to be dependable. Temperature verification and temperature calibration for ISO and GLP practices are quickly and easily performed with optional accessories including NIST traceable dual thermocouples and calibration source instruments.

 

Phoenix satisfies the equipment requirements for "electrically heated" furnaces in the following methods:

* ASTM, USP (281 - ROI & 733-LOI), AOAC, FDA, ISO & DIN

Phoenix also meets the requirements for applications listing a "microwave-heated" furnace

* ASTM D5630-94, ASTM D1506-94b

 

Workstation

All Phoenix Microwave Muffle Furnace Systems are available with workstation options including a balance and printer.

The Phoenix Workstation option transforms your microwave muffle furnace into a complete center for accurate ashing and data compilation. The system utilizes the furnace’s built-in serial and parallel ports to connect to a balance for weighing and a printer for complete documentation of the ashing process to assist you in complying with ISO and other QC requirements.

The Phoenix Workstation uses a 100 g balance with 0.0001 g sensitivity for sample weighing. The balance communicates directly with the Phoenix furnace by a RS-232 port, which is a standard feature in every CEM muffle furnace. Once the sample has completed the ashing process and has been reweighed, the user can choose to print the sample results and information with the Workstation’s printer.

 

Phoenix Features

Fast & Efficient
Phoenix Microwave Muffle Furnaces perform many high temperature applications up to 97% faster than traditional muffle furnaces, giving you more time to make adjustments to your process and reduce out-of-specification product.


Safe
Phoenix reduces exposure to fumes and heat with a built-in exhaust system that does not require fume hood space. These rugged, durable furnaces features door interlocks and built-in system diagnostics.

Accurate
Phoenix Microwave Muffle Furnaces satisfy standard methods that require electrically heated furnaces. They have built-in calibration software and NIST traceable accessories are available.


Easy-to-Use
Auto-start software allows pre-programmable warm-up and shut down. Phoenix Microwave Muffle Furnaces store up to 20 user-programmed methods.

 

Phoenix Sulfated Ashing

Ash pharmaceutical raw materials, excipients and finished products in minutes, while safely removing and neutralizing sulfur dioxide and nitric acid emissions to meet ISO 14000 regulations. The Phoenix Microwave Sulfated Ashing Option features a vapor scrubber system to safely remove harmful fumes from the furnace cavity and neutralize any residual acid exhausted from the sulfated ashing process.

  • Meets requirements for USP 281 (ROI) & USP 733 (LOI)
  • Built-in serial and parallel ports provide full documentation of method, completion date, and time
  • Menu-driven software permits simple entry and storage of operating parameters for up to 20 methods
  • Rapid disconnect feature allows system to be used as either a standard ashing system or a sulfated ashing system in less than 5 minutes without the use of tools
  • Quartz furnace ceiling assures sample purity
  • Easy-to-use
  • Available as a workstation with balance and printer


Temperature verification and temperature calibration for ISO and GLP practices are quickly and easily performed with optionalaccessories including NIST traceable dual thermocouples and calibration source instruments.

 

Phoenix Airwave

The Phoenix Airwave Microwave Muffle Furnace meets the most demanding requirements of large organic samples with ease. This microwave muffle furnace utilizes a patented air amplified exhaust system to quickly and safely ash samples, removing large quantities of air and volatile by-products.

Legendary power at your fingertips!

  • Fast, accurate, easy-to-use
  • Eliminates the need for volume reduction/carbonization on a Bunsen burner or hot plate
  • Exhaust 130 CFM or more of air per minute (adjustable)
  • Volume reduction of large samples in minutes by high-speed evaporation
  • Increased airflow accelerates oxidation of samples


The Phoenix Airwave Microwave Muffle Furnace is available with your choice of either a High Temperature or High Capacity furnace. The High Temperature furnaces reach 1,200 °C and can process up to eight 25-mL crucibles. For laboratories needing greater throughput, the High Capacity furnaces reach 1,000 °C and hold up to fifteen 25-mL crucibles. Any crucible that can be used in a conventional muffle furnace (including platinum) can also be used in the Phoenix Microwave Ashing Systems.

Standard features include:

  • Programmable temperature control
  • Auto-Start/Auto-Shutdown software
  • Built-in exhaust system
  • Entry and storage of up to 20 methods
  • Built-in calibration software
  • Over-temperature and thermocouple failure safeguards
  • Built-in system diagnostics
  • Use any type of crucible normally used in a conventional muffle furnace, including platinum!
  • Available as a workstation with balance and printer


The Phoenix Airwave Microwave Muffle Furnace can perform many high temperature applications up to 97% faster than conventional muffle furnaces. The system is rugged and engineered to be dependable. Temperature verification and temperature calibration for ISO and GLP practices are quickly and easily performed with optional accessories including NIST traceable dual thermocouples and calibration source instruments.

 

Phoenix Bone Content Analysis

Direct bone content analysis in less than 15 minutes!

Forget titrations and back calculations for bone content! Get a fast, accurate and direct bone content analysis with the PhoenixMicrowave Furnace. Save money and increase production yields by running closer to target!
 

Phoenix™ 
for Bone Content Analysis

  • Direct method
  • More accurate than titration
  • No chemicals
  • Accurate bone content in less than 15 minutes!
  • Automatically calculates results

 

Bone Content Results: Mechanically Separated Chicken (MSC)

Sample % Bone AOAC Bone Difference
1 0.77 0.83 -0.06
2 0.70 0.76 -0.06
3 0.80 0.62 0.18
4 0.86 0.51 0.35
5 0.59 0.55 0.04
6 0.64 0.56 0.08
7 0.79 0.50 0.29
8 0.50 0.50 0
9 0.83 0.85 -0.02
10 0.85 0.88 -0.03

 

Phoenix Accessories 

CEM offers accessories for the calibration and verification of the temperature control circuitry to meet governmental regulations for various applications.

 

Improve Results with Quartz Fiber Crucibles 

CEM’s unique, patented quartz fiber crucibles dramatically reduce ashing times and cool in seconds. The quartz fiber material allows oxygen to circulate around the sample speeding combustion even with our unique crucible caps in place. 

  • Reduce analysis time by as much as 97%!
  • Cools in seconds
  • No need for desiccation
  • Speeds sample oxidation using a flow through advanced material design
  • Withstands temperatures up to 1,000 °C
  • Unbreakable


Crucible caps can be used with our 50- or 100-ml crucibles. Try them out next time you have to ash a sample that needs to be contained. 

Ideal for low ash samples and samples with high organic content

  • Contains the sample when ignition occurs
  • Reduces contamination
  • Improves accuracy on ROI and LOI determinations

 

Automatic replenishment programs, yearly contracts and volume pricing are available for quartz fiber crucibles. For more information and part numbers, please visit our Consumables page.

 

Self-Sealing Quartz Crucibles 
For oxygen-free ashing, self-sealing quartz crucibles are available. These crucibles can be used for Carbon Black determination in polyethylene and polypropylene and eliminate the need for slow, fragile tube furnaces.

 

Ashing under Inert Gas *
The super-fast muffle furnace allows the rapid determination of soot and carbon fibers and carbon nanotubes in polymers

The Phoenix can be used as a rapid plastic incinerator with inert gas atmosphere. This enables the rapid ashing of a variety of different plastics and rubbers, for the determination of soot or carbon content and the content of carbon nanotubes. The result: What previously took hours, is now achieved in minutes. The application areas for such plastics compounds are typically in the aircraft and automobile (bumpers, moldings, fittings, sinks, counter tops, finished parts, etc.) amongst others.

Since the material properties of plastic compounds depend essentially on its filler content, a rapid determination of this filler (carbon black, carbon fiber, carbon nanotubes, etc.) is required for an effective process control. Substantial cost savings can be made by a quick intervention in the current production process. With a conventional muffle furnace, polymer and filler are incinerated together in a crucible and thus the filler cannot be measured. The alternative is to use the Phoenix with an inert gas atmosphere such as a nitrogen purge.

Results are obtained in just 10 minutes. The heating muffle is purged with an inert gas such as nitrogen. The plastic polymer is carbonized and exits the crucible but the carbon-containing filler in the crucible remains. The built-in fan removes smoke, heat and fumes automatically, thus increasing the active safety at work.

 

Material Science
The inert gas option can also be used in a variety of applications related to material science. Various publications have highlighted the benefits of using microwave energy and we can now offer a solution for reactions requiring an inert atmosphere.
Microwave irradiation quickly applies the energy necessary to achieve high temperatures, enabling reactions to be performed quickly and efficiently. The instant power on / power off provides for a steep rise in temperature during the heating but also for a steep decline during the cooling resulting in high quality materials.

 

Microwave energy has been used for making materials such as: 
 

Quantum Dots
Zeolites
Metal Oxides

Metal Organic Frameworks
Gold, silver, and other metal nanomaterials
Nanocomposite materials

Nitride powders
Lithium ion materials



*CEM cannot fully guarantee an oxygen-free environment using this process.

 

Calibration Source Instrument (NIST traceable) 
The calibration source instrument and built-in system software allow rapid calibration of the temperature control circuitry of the Phoenix Microwave Ashing Systems. A NIST traceable certificate of calibration is supplied with the instrument.

 

Dual Element Thermocouple (NIST traceable) 
The type K Dual Element Thermocouple contains two thermocouples in one sheath. While one thermocouple controls the operating temperature, the second thermocouple can be connected to a digital thermometer to verify the accuracy of the controlling thermocouple. It is NIST traceable with a certificate of calibration. 

 

Cooling Fan 
The furnace cooling fan rapidly reduces heat to the starting temperature.

 

All Phoenix Microwave Ashing Systems are available with workstation options including a balance and printer. 

 

The Phoenix consists of a 1400 W microwave heating system containing a 5.0 liter (300 in3) chamber which can be heated to 1000 °C or a 1.8 liter (112.5 in3) chamber which can be heat to 1200 °C using microwave energy. The unit maintains 2.8 m(100 ft3) of air flow per minute through the microwave cavity to rapidly ash materials and remove combustion by-products. Internal temperature calibration software. Includes integral dual thermocouple Temperature Control System for either single set-point temperature or eight segmented ramping temperature control programs. Program storing, processing and reporting weight data and % Ash, % LOI, % ROI, % LOD, %Fixed, %Volatile and %Total Residue to the instrument display, printer or external computer.  Two RS232C 9-pin serial interfaces for option balance and external computer; one 25-pin parallel port for optional printer.  Accessory Starter Kit includes: 8 ft. exhaust hose with connector, clamp 90 degree elbow. (20) 20 mL & (4) 50 mL Quartz Fiber Ashing Crucibles, (4) 50 mL crucibles and 200 ashing disks, spare fuses, thermocouple, pedestal access tool, power cord and operation manual. Manufactured by CEM Corporation, ISO-9001 certified. 

Phoenix Microwave Ashing System

OVERVIEW
DOWNLOADS
Brand: CEM
Part No: PHOENIX
Availability: 6-8 weeks

Speed, Capacity, Versatility

Phoenix
Microwave
Muffle 
Furnace

 

Precise Results in Seconds

 

The Phoenix line of microwave muffle furnaces offers unmatched versatility and speed in a rugged, easy-to-use system. Choose from two configurations and a variety of options!
 

Legendary power at your fingertips!
 

  • Convenience - Accurate results in minutes
  • Speed - Up to 10 times faster than conventional muffle furnaces
  • Capacity - Ash up to 15 samples at one time
  • Versatility - Use any type of crucible normally used in conventional ashing systems, even platinum


The Phoenix Microwave Muffle Furnace System is available with your choice of either a High Temperature or High Capacity furnace. The High Temperature furnaces reach 1,200 °C and can process up to eight 25-mL crucibles. For laboratories needing greater throughput, the High Capacity furnaces reach 1,000°C and hold up to fifteen 25-mL crucibles. Any crucible that can be used in a conventional muffle furnace (including platinum) can also be used in the Phoenix Microwave Muffle Furnace Systems.

 

Phoenix™ Microwave Muffle Furnace

The Phoenix Microwave Muffle Furnaces enable companies in many diverse industries to improve their process control, allowing them to make rapid adjustments to reduce "out-of-specification" product. These systems can perform many high temperature applications up to 97% faster than traditional muffle furnaces. The standard Phoenix Microwave Muffle Furnace configuration features:
 

  • Programmable temperature control
  • Auto-Start/Auto-Shutdown software
  • Built-in exhaust system
  • Entry and storage of up to 20 methods
  • Built-in calibration software
  • Over-temperature and thermocouple failure safeguards
  • Built-in system diagnostics
  • Use any type of crucible normally used in a conventional muffle furnace, including platinum!


The Phoenix Microwave Muffle Furnace Systems are rugged, easy-to-use and engineered to be dependable. Temperature verification and temperature calibration for ISO and GLP practices are quickly and easily performed with optional accessories including NIST traceable dual thermocouples and calibration source instruments.

 

Phoenix satisfies the equipment requirements for "electrically heated" furnaces in the following methods:

* ASTM, USP (281 - ROI & 733-LOI), AOAC, FDA, ISO & DIN

Phoenix also meets the requirements for applications listing a "microwave-heated" furnace

* ASTM D5630-94, ASTM D1506-94b

 

Workstation

All Phoenix Microwave Muffle Furnace Systems are available with workstation options including a balance and printer.

The Phoenix Workstation option transforms your microwave muffle furnace into a complete center for accurate ashing and data compilation. The system utilizes the furnace’s built-in serial and parallel ports to connect to a balance for weighing and a printer for complete documentation of the ashing process to assist you in complying with ISO and other QC requirements.

The Phoenix Workstation uses a 100 g balance with 0.0001 g sensitivity for sample weighing. The balance communicates directly with the Phoenix furnace by a RS-232 port, which is a standard feature in every CEM muffle furnace. Once the sample has completed the ashing process and has been reweighed, the user can choose to print the sample results and information with the Workstation’s printer.

 

Phoenix Features

Fast & Efficient
Phoenix Microwave Muffle Furnaces perform many high temperature applications up to 97% faster than traditional muffle furnaces, giving you more time to make adjustments to your process and reduce out-of-specification product.


Safe
Phoenix reduces exposure to fumes and heat with a built-in exhaust system that does not require fume hood space. These rugged, durable furnaces features door interlocks and built-in system diagnostics.

Accurate
Phoenix Microwave Muffle Furnaces satisfy standard methods that require electrically heated furnaces. They have built-in calibration software and NIST traceable accessories are available.


Easy-to-Use
Auto-start software allows pre-programmable warm-up and shut down. Phoenix Microwave Muffle Furnaces store up to 20 user-programmed methods.

 

Phoenix Sulfated Ashing

Ash pharmaceutical raw materials, excipients and finished products in minutes, while safely removing and neutralizing sulfur dioxide and nitric acid emissions to meet ISO 14000 regulations. The Phoenix Microwave Sulfated Ashing Option features a vapor scrubber system to safely remove harmful fumes from the furnace cavity and neutralize any residual acid exhausted from the sulfated ashing process.

  • Meets requirements for USP 281 (ROI) & USP 733 (LOI)
  • Built-in serial and parallel ports provide full documentation of method, completion date, and time
  • Menu-driven software permits simple entry and storage of operating parameters for up to 20 methods
  • Rapid disconnect feature allows system to be used as either a standard ashing system or a sulfated ashing system in less than 5 minutes without the use of tools
  • Quartz furnace ceiling assures sample purity
  • Easy-to-use
  • Available as a workstation with balance and printer


Temperature verification and temperature calibration for ISO and GLP practices are quickly and easily performed with optionalaccessories including NIST traceable dual thermocouples and calibration source instruments.

 

Phoenix Airwave

The Phoenix Airwave Microwave Muffle Furnace meets the most demanding requirements of large organic samples with ease. This microwave muffle furnace utilizes a patented air amplified exhaust system to quickly and safely ash samples, removing large quantities of air and volatile by-products.

Legendary power at your fingertips!

  • Fast, accurate, easy-to-use
  • Eliminates the need for volume reduction/carbonization on a Bunsen burner or hot plate
  • Exhaust 130 CFM or more of air per minute (adjustable)
  • Volume reduction of large samples in minutes by high-speed evaporation
  • Increased airflow accelerates oxidation of samples


The Phoenix Airwave Microwave Muffle Furnace is available with your choice of either a High Temperature or High Capacity furnace. The High Temperature furnaces reach 1,200 °C and can process up to eight 25-mL crucibles. For laboratories needing greater throughput, the High Capacity furnaces reach 1,000 °C and hold up to fifteen 25-mL crucibles. Any crucible that can be used in a conventional muffle furnace (including platinum) can also be used in the Phoenix Microwave Ashing Systems.

Standard features include:

  • Programmable temperature control
  • Auto-Start/Auto-Shutdown software
  • Built-in exhaust system
  • Entry and storage of up to 20 methods
  • Built-in calibration software
  • Over-temperature and thermocouple failure safeguards
  • Built-in system diagnostics
  • Use any type of crucible normally used in a conventional muffle furnace, including platinum!
  • Available as a workstation with balance and printer


The Phoenix Airwave Microwave Muffle Furnace can perform many high temperature applications up to 97% faster than conventional muffle furnaces. The system is rugged and engineered to be dependable. Temperature verification and temperature calibration for ISO and GLP practices are quickly and easily performed with optional accessories including NIST traceable dual thermocouples and calibration source instruments.

 

Phoenix Bone Content Analysis

Direct bone content analysis in less than 15 minutes!

Forget titrations and back calculations for bone content! Get a fast, accurate and direct bone content analysis with the PhoenixMicrowave Furnace. Save money and increase production yields by running closer to target!
 

Phoenix™ 
for Bone Content Analysis

  • Direct method
  • More accurate than titration
  • No chemicals
  • Accurate bone content in less than 15 minutes!
  • Automatically calculates results

 

Bone Content Results: Mechanically Separated Chicken (MSC)

Sample % Bone AOAC Bone Difference
1 0.77 0.83 -0.06
2 0.70 0.76 -0.06
3 0.80 0.62 0.18
4 0.86 0.51 0.35
5 0.59 0.55 0.04
6 0.64 0.56 0.08
7 0.79 0.50 0.29
8 0.50 0.50 0
9 0.83 0.85 -0.02
10 0.85 0.88 -0.03

 

Phoenix Accessories 

CEM offers accessories for the calibration and verification of the temperature control circuitry to meet governmental regulations for various applications.

 

Improve Results with Quartz Fiber Crucibles 

CEM’s unique, patented quartz fiber crucibles dramatically reduce ashing times and cool in seconds. The quartz fiber material allows oxygen to circulate around the sample speeding combustion even with our unique crucible caps in place. 

  • Reduce analysis time by as much as 97%!
  • Cools in seconds
  • No need for desiccation
  • Speeds sample oxidation using a flow through advanced material design
  • Withstands temperatures up to 1,000 °C
  • Unbreakable


Crucible caps can be used with our 50- or 100-ml crucibles. Try them out next time you have to ash a sample that needs to be contained. 

Ideal for low ash samples and samples with high organic content

  • Contains the sample when ignition occurs
  • Reduces contamination
  • Improves accuracy on ROI and LOI determinations

 

Automatic replenishment programs, yearly contracts and volume pricing are available for quartz fiber crucibles. For more information and part numbers, please visit our Consumables page.

 

Self-Sealing Quartz Crucibles 
For oxygen-free ashing, self-sealing quartz crucibles are available. These crucibles can be used for Carbon Black determination in polyethylene and polypropylene and eliminate the need for slow, fragile tube furnaces.

 

Ashing under Inert Gas *
The super-fast muffle furnace allows the rapid determination of soot and carbon fibers and carbon nanotubes in polymers

The Phoenix can be used as a rapid plastic incinerator with inert gas atmosphere. This enables the rapid ashing of a variety of different plastics and rubbers, for the determination of soot or carbon content and the content of carbon nanotubes. The result: What previously took hours, is now achieved in minutes. The application areas for such plastics compounds are typically in the aircraft and automobile (bumpers, moldings, fittings, sinks, counter tops, finished parts, etc.) amongst others.

Since the material properties of plastic compounds depend essentially on its filler content, a rapid determination of this filler (carbon black, carbon fiber, carbon nanotubes, etc.) is required for an effective process control. Substantial cost savings can be made by a quick intervention in the current production process. With a conventional muffle furnace, polymer and filler are incinerated together in a crucible and thus the filler cannot be measured. The alternative is to use the Phoenix with an inert gas atmosphere such as a nitrogen purge.

Results are obtained in just 10 minutes. The heating muffle is purged with an inert gas such as nitrogen. The plastic polymer is carbonized and exits the crucible but the carbon-containing filler in the crucible remains. The built-in fan removes smoke, heat and fumes automatically, thus increasing the active safety at work.

 

Material Science
The inert gas option can also be used in a variety of applications related to material science. Various publications have highlighted the benefits of using microwave energy and we can now offer a solution for reactions requiring an inert atmosphere.
Microwave irradiation quickly applies the energy necessary to achieve high temperatures, enabling reactions to be performed quickly and efficiently. The instant power on / power off provides for a steep rise in temperature during the heating but also for a steep decline during the cooling resulting in high quality materials.

 

Microwave energy has been used for making materials such as: 
 

Quantum Dots
Zeolites
Metal Oxides

Metal Organic Frameworks
Gold, silver, and other metal nanomaterials
Nanocomposite materials

Nitride powders
Lithium ion materials



*CEM cannot fully guarantee an oxygen-free environment using this process.

 

Calibration Source Instrument (NIST traceable) 
The calibration source instrument and built-in system software allow rapid calibration of the temperature control circuitry of the Phoenix Microwave Ashing Systems. A NIST traceable certificate of calibration is supplied with the instrument.

 

Dual Element Thermocouple (NIST traceable) 
The type K Dual Element Thermocouple contains two thermocouples in one sheath. While one thermocouple controls the operating temperature, the second thermocouple can be connected to a digital thermometer to verify the accuracy of the controlling thermocouple. It is NIST traceable with a certificate of calibration. 

 

Cooling Fan 
The furnace cooling fan rapidly reduces heat to the starting temperature.

 

All Phoenix Microwave Ashing Systems are available with workstation options including a balance and printer. 

 

The Phoenix consists of a 1400 W microwave heating system containing a 5.0 liter (300 in3) chamber which can be heated to 1000 °C or a 1.8 liter (112.5 in3) chamber which can be heat to 1200 °C using microwave energy. The unit maintains 2.8 m(100 ft3) of air flow per minute through the microwave cavity to rapidly ash materials and remove combustion by-products. Internal temperature calibration software. Includes integral dual thermocouple Temperature Control System for either single set-point temperature or eight segmented ramping temperature control programs. Program storing, processing and reporting weight data and % Ash, % LOI, % ROI, % LOD, %Fixed, %Volatile and %Total Residue to the instrument display, printer or external computer.  Two RS232C 9-pin serial interfaces for option balance and external computer; one 25-pin parallel port for optional printer.  Accessory Starter Kit includes: 8 ft. exhaust hose with connector, clamp 90 degree elbow. (20) 20 mL & (4) 50 mL Quartz Fiber Ashing Crucibles, (4) 50 mL crucibles and 200 ashing disks, spare fuses, thermocouple, pedestal access tool, power cord and operation manual. Manufactured by CEM Corporation, ISO-9001 certified. 

OVERVIEW
DOWNLOADS
Brand: CEM
Part No: PHOENIX
Availability: 6-8 weeks

Speed, Capacity, Versatility

Phoenix
Microwave
Muffle 
Furnace

 

Precise Results in Seconds

 

The Phoenix line of microwave muffle furnaces offers unmatched versatility and speed in a rugged, easy-to-use system. Choose from two configurations and a variety of options!
 

Legendary power at your fingertips!
 

  • Convenience - Accurate results in minutes
  • Speed - Up to 10 times faster than conventional muffle furnaces
  • Capacity - Ash up to 15 samples at one time
  • Versatility - Use any type of crucible normally used in conventional ashing systems, even platinum


The Phoenix Microwave Muffle Furnace System is available with your choice of either a High Temperature or High Capacity furnace. The High Temperature furnaces reach 1,200 °C and can process up to eight 25-mL crucibles. For laboratories needing greater throughput, the High Capacity furnaces reach 1,000°C and hold up to fifteen 25-mL crucibles. Any crucible that can be used in a conventional muffle furnace (including platinum) can also be used in the Phoenix Microwave Muffle Furnace Systems.

 

Phoenix™ Microwave Muffle Furnace

The Phoenix Microwave Muffle Furnaces enable companies in many diverse industries to improve their process control, allowing them to make rapid adjustments to reduce "out-of-specification" product. These systems can perform many high temperature applications up to 97% faster than traditional muffle furnaces. The standard Phoenix Microwave Muffle Furnace configuration features:
 

  • Programmable temperature control
  • Auto-Start/Auto-Shutdown software
  • Built-in exhaust system
  • Entry and storage of up to 20 methods
  • Built-in calibration software
  • Over-temperature and thermocouple failure safeguards
  • Built-in system diagnostics
  • Use any type of crucible normally used in a conventional muffle furnace, including platinum!


The Phoenix Microwave Muffle Furnace Systems are rugged, easy-to-use and engineered to be dependable. Temperature verification and temperature calibration for ISO and GLP practices are quickly and easily performed with optional accessories including NIST traceable dual thermocouples and calibration source instruments.

 

Phoenix satisfies the equipment requirements for "electrically heated" furnaces in the following methods:

* ASTM, USP (281 - ROI & 733-LOI), AOAC, FDA, ISO & DIN

Phoenix also meets the requirements for applications listing a "microwave-heated" furnace

* ASTM D5630-94, ASTM D1506-94b

 

Workstation

All Phoenix Microwave Muffle Furnace Systems are available with workstation options including a balance and printer.

The Phoenix Workstation option transforms your microwave muffle furnace into a complete center for accurate ashing and data compilation. The system utilizes the furnace’s built-in serial and parallel ports to connect to a balance for weighing and a printer for complete documentation of the ashing process to assist you in complying with ISO and other QC requirements.

The Phoenix Workstation uses a 100 g balance with 0.0001 g sensitivity for sample weighing. The balance communicates directly with the Phoenix furnace by a RS-232 port, which is a standard feature in every CEM muffle furnace. Once the sample has completed the ashing process and has been reweighed, the user can choose to print the sample results and information with the Workstation’s printer.

 

Phoenix Features

Fast & Efficient
Phoenix Microwave Muffle Furnaces perform many high temperature applications up to 97% faster than traditional muffle furnaces, giving you more time to make adjustments to your process and reduce out-of-specification product.


Safe
Phoenix reduces exposure to fumes and heat with a built-in exhaust system that does not require fume hood space. These rugged, durable furnaces features door interlocks and built-in system diagnostics.

Accurate
Phoenix Microwave Muffle Furnaces satisfy standard methods that require electrically heated furnaces. They have built-in calibration software and NIST traceable accessories are available.


Easy-to-Use
Auto-start software allows pre-programmable warm-up and shut down. Phoenix Microwave Muffle Furnaces store up to 20 user-programmed methods.

 

Phoenix Sulfated Ashing

Ash pharmaceutical raw materials, excipients and finished products in minutes, while safely removing and neutralizing sulfur dioxide and nitric acid emissions to meet ISO 14000 regulations. The Phoenix Microwave Sulfated Ashing Option features a vapor scrubber system to safely remove harmful fumes from the furnace cavity and neutralize any residual acid exhausted from the sulfated ashing process.

  • Meets requirements for USP 281 (ROI) & USP 733 (LOI)
  • Built-in serial and parallel ports provide full documentation of method, completion date, and time
  • Menu-driven software permits simple entry and storage of operating parameters for up to 20 methods
  • Rapid disconnect feature allows system to be used as either a standard ashing system or a sulfated ashing system in less than 5 minutes without the use of tools
  • Quartz furnace ceiling assures sample purity
  • Easy-to-use
  • Available as a workstation with balance and printer


Temperature verification and temperature calibration for ISO and GLP practices are quickly and easily performed with optionalaccessories including NIST traceable dual thermocouples and calibration source instruments.

 

Phoenix Airwave

The Phoenix Airwave Microwave Muffle Furnace meets the most demanding requirements of large organic samples with ease. This microwave muffle furnace utilizes a patented air amplified exhaust system to quickly and safely ash samples, removing large quantities of air and volatile by-products.

Legendary power at your fingertips!

  • Fast, accurate, easy-to-use
  • Eliminates the need for volume reduction/carbonization on a Bunsen burner or hot plate
  • Exhaust 130 CFM or more of air per minute (adjustable)
  • Volume reduction of large samples in minutes by high-speed evaporation
  • Increased airflow accelerates oxidation of samples


The Phoenix Airwave Microwave Muffle Furnace is available with your choice of either a High Temperature or High Capacity furnace. The High Temperature furnaces reach 1,200 °C and can process up to eight 25-mL crucibles. For laboratories needing greater throughput, the High Capacity furnaces reach 1,000 °C and hold up to fifteen 25-mL crucibles. Any crucible that can be used in a conventional muffle furnace (including platinum) can also be used in the Phoenix Microwave Ashing Systems.

Standard features include:

  • Programmable temperature control
  • Auto-Start/Auto-Shutdown software
  • Built-in exhaust system
  • Entry and storage of up to 20 methods
  • Built-in calibration software
  • Over-temperature and thermocouple failure safeguards
  • Built-in system diagnostics
  • Use any type of crucible normally used in a conventional muffle furnace, including platinum!
  • Available as a workstation with balance and printer


The Phoenix Airwave Microwave Muffle Furnace can perform many high temperature applications up to 97% faster than conventional muffle furnaces. The system is rugged and engineered to be dependable. Temperature verification and temperature calibration for ISO and GLP practices are quickly and easily performed with optional accessories including NIST traceable dual thermocouples and calibration source instruments.

 

Phoenix Bone Content Analysis

Direct bone content analysis in less than 15 minutes!

Forget titrations and back calculations for bone content! Get a fast, accurate and direct bone content analysis with the PhoenixMicrowave Furnace. Save money and increase production yields by running closer to target!
 

Phoenix™ 
for Bone Content Analysis

  • Direct method
  • More accurate than titration
  • No chemicals
  • Accurate bone content in less than 15 minutes!
  • Automatically calculates results

 

Bone Content Results: Mechanically Separated Chicken (MSC)

Sample % Bone AOAC Bone Difference
1 0.77 0.83 -0.06
2 0.70 0.76 -0.06
3 0.80 0.62 0.18
4 0.86 0.51 0.35
5 0.59 0.55 0.04
6 0.64 0.56 0.08
7 0.79 0.50 0.29
8 0.50 0.50 0
9 0.83 0.85 -0.02
10 0.85 0.88 -0.03

 

Phoenix Accessories 

CEM offers accessories for the calibration and verification of the temperature control circuitry to meet governmental regulations for various applications.

 

Improve Results with Quartz Fiber Crucibles 

CEM’s unique, patented quartz fiber crucibles dramatically reduce ashing times and cool in seconds. The quartz fiber material allows oxygen to circulate around the sample speeding combustion even with our unique crucible caps in place. 

  • Reduce analysis time by as much as 97%!
  • Cools in seconds
  • No need for desiccation
  • Speeds sample oxidation using a flow through advanced material design
  • Withstands temperatures up to 1,000 °C
  • Unbreakable


Crucible caps can be used with our 50- or 100-ml crucibles. Try them out next time you have to ash a sample that needs to be contained. 

Ideal for low ash samples and samples with high organic content

  • Contains the sample when ignition occurs
  • Reduces contamination
  • Improves accuracy on ROI and LOI determinations

 

Automatic replenishment programs, yearly contracts and volume pricing are available for quartz fiber crucibles. For more information and part numbers, please visit our Consumables page.

 

Self-Sealing Quartz Crucibles 
For oxygen-free ashing, self-sealing quartz crucibles are available. These crucibles can be used for Carbon Black determination in polyethylene and polypropylene and eliminate the need for slow, fragile tube furnaces.

 

Ashing under Inert Gas *
The super-fast muffle furnace allows the rapid determination of soot and carbon fibers and carbon nanotubes in polymers

The Phoenix can be used as a rapid plastic incinerator with inert gas atmosphere. This enables the rapid ashing of a variety of different plastics and rubbers, for the determination of soot or carbon content and the content of carbon nanotubes. The result: What previously took hours, is now achieved in minutes. The application areas for such plastics compounds are typically in the aircraft and automobile (bumpers, moldings, fittings, sinks, counter tops, finished parts, etc.) amongst others.

Since the material properties of plastic compounds depend essentially on its filler content, a rapid determination of this filler (carbon black, carbon fiber, carbon nanotubes, etc.) is required for an effective process control. Substantial cost savings can be made by a quick intervention in the current production process. With a conventional muffle furnace, polymer and filler are incinerated together in a crucible and thus the filler cannot be measured. The alternative is to use the Phoenix with an inert gas atmosphere such as a nitrogen purge.

Results are obtained in just 10 minutes. The heating muffle is purged with an inert gas such as nitrogen. The plastic polymer is carbonized and exits the crucible but the carbon-containing filler in the crucible remains. The built-in fan removes smoke, heat and fumes automatically, thus increasing the active safety at work.

 

Material Science
The inert gas option can also be used in a variety of applications related to material science. Various publications have highlighted the benefits of using microwave energy and we can now offer a solution for reactions requiring an inert atmosphere.
Microwave irradiation quickly applies the energy necessary to achieve high temperatures, enabling reactions to be performed quickly and efficiently. The instant power on / power off provides for a steep rise in temperature during the heating but also for a steep decline during the cooling resulting in high quality materials.

 

Microwave energy has been used for making materials such as: 
 

Quantum Dots
Zeolites
Metal Oxides

Metal Organic Frameworks
Gold, silver, and other metal nanomaterials
Nanocomposite materials

Nitride powders
Lithium ion materials



*CEM cannot fully guarantee an oxygen-free environment using this process.

 

Calibration Source Instrument (NIST traceable) 
The calibration source instrument and built-in system software allow rapid calibration of the temperature control circuitry of the Phoenix Microwave Ashing Systems. A NIST traceable certificate of calibration is supplied with the instrument.

 

Dual Element Thermocouple (NIST traceable) 
The type K Dual Element Thermocouple contains two thermocouples in one sheath. While one thermocouple controls the operating temperature, the second thermocouple can be connected to a digital thermometer to verify the accuracy of the controlling thermocouple. It is NIST traceable with a certificate of calibration. 

 

Cooling Fan 
The furnace cooling fan rapidly reduces heat to the starting temperature.

 

All Phoenix Microwave Ashing Systems are available with workstation options including a balance and printer. 

 

The Phoenix consists of a 1400 W microwave heating system containing a 5.0 liter (300 in3) chamber which can be heated to 1000 °C or a 1.8 liter (112.5 in3) chamber which can be heat to 1200 °C using microwave energy. The unit maintains 2.8 m(100 ft3) of air flow per minute through the microwave cavity to rapidly ash materials and remove combustion by-products. Internal temperature calibration software. Includes integral dual thermocouple Temperature Control System for either single set-point temperature or eight segmented ramping temperature control programs. Program storing, processing and reporting weight data and % Ash, % LOI, % ROI, % LOD, %Fixed, %Volatile and %Total Residue to the instrument display, printer or external computer.  Two RS232C 9-pin serial interfaces for option balance and external computer; one 25-pin parallel port for optional printer.  Accessory Starter Kit includes: 8 ft. exhaust hose with connector, clamp 90 degree elbow. (20) 20 mL & (4) 50 mL Quartz Fiber Ashing Crucibles, (4) 50 mL crucibles and 200 ashing disks, spare fuses, thermocouple, pedestal access tool, power cord and operation manual. Manufactured by CEM Corporation, ISO-9001 certified. 

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